{"id":302886,"date":"2024-10-19T20:41:54","date_gmt":"2024-10-19T20:41:54","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bsi-pd-iec-ts-62607-4-82020\/"},"modified":"2024-10-25T18:13:44","modified_gmt":"2024-10-25T18:13:44","slug":"bsi-pd-iec-ts-62607-4-82020","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bsi-pd-iec-ts-62607-4-82020\/","title":{"rendered":"BSI PD IEC TS 62607-4-8:2020"},"content":{"rendered":"<p>This part of IEC 62607, which is a Technical Specification, specifies a test method for the determination of water content in electrode nanomaterials for nano-enabled electrical energy storage devices, using the Karl Fischer coulometric titration method.<\/p>\n<p>This document includes:<\/p>\n<ul>\n<li>\n<p>recommendations for sample preparation,<\/p>\n<\/li>\n<li>\n<p>outlines of the experimental procedures used to measure electrode nanomaterial properties, and<\/p>\n<\/li>\n<li>\n<p>methods of interpretation of results and discussion of data analysis.<\/p>\n<\/li>\n<\/ul>\n<blockquote>\n<p>NOTE This method has precision as low as 0,000 1 %. The best applicable measure range is 0,01 % to 1 %.<\/p>\n<\/blockquote>\n<p>This document is not applicable for samples that can react with the main components of Karl Fischer reagent and produce water, or samples that can react with iodine or iodide ion.<\/p>\n<h4>PDF Catalog<\/h4>\n<table border=\"1px\" class=\"des-table\">\n<tr>\n<th>PDF Pages<\/th>\n<th>PDF Title<\/th>\n<\/tr>\n<tr>\n<td><b>2<b><\/td>\n<td>undefined  <\/td>\n<\/tr>\n<tr>\n<td><b>4<b><\/td>\n<td>CONTENTS  <\/td>\n<\/tr>\n<tr>\n<td><b>6<b><\/td>\n<td>FOREWORD  <\/td>\n<\/tr>\n<tr>\n<td><b>8<b><\/td>\n<td>INTRODUCTION  <\/td>\n<\/tr>\n<tr>\n<td><b>9<b><\/td>\n<td>1 Scope <br \/> 2 Normative references <br \/> 3 Terms and definitions  <\/td>\n<\/tr>\n<tr>\n<td><b>10<b><\/td>\n<td>4 Principle   <\/td>\n<\/tr>\n<tr>\n<td><b>11<b><\/td>\n<td>5 Reagents <br \/> 5.1 Coulometric Karl Fischer reagent <br \/> 5.2 Methanol (anhydrous) <br \/> 5.3 Carrier gas <br \/> 5.4 Water standard for Karl Fischer coulometric titration <br \/> 6 Apparatus <br \/> 6.1 Karl Fischer coulometric titration apparatus <br \/> 6.2 Evaporator  <\/td>\n<\/tr>\n<tr>\n<td><b>12<b><\/td>\n<td>6.3 Analytical balance <br \/> 6.4 Sample container <br \/> 6.5 Micro-syringe <br \/> 6.6 Dew-point hygrometer <br \/> 7 Sample handling and sampling <br \/> 7.1 Sample handling <br \/> Figures <br \/> Figure 1 \u2013 Example of Karl Fischer coulometric titration apparatus and evaporator  <\/td>\n<\/tr>\n<tr>\n<td><b>13<b><\/td>\n<td>7.2 Sampling <br \/> 8 Procedure <br \/> 8.1 Maintenance <br \/> 8.1.1 Reagent change <br \/> 8.1.2 Cleaning <br \/> 8.1.3 Calibration <br \/> 8.2 Measurement steps <br \/> Tables <br \/> Table 1 \u2013 Sample mass against water to be determined  <\/td>\n<\/tr>\n<tr>\n<td><b>14<b><\/td>\n<td>8.3 Water content of the sample  <\/td>\n<\/tr>\n<tr>\n<td><b>15<b><\/td>\n<td>9 Precision <br \/> 9.1 General <br \/> 9.2 Repeatability <br \/> 9.3 Reproducibility <br \/> 10 Test report  <\/td>\n<\/tr>\n<tr>\n<td><b>16<b><\/td>\n<td>Annex A (informative)Case study <br \/> A.1 General <br \/> A.2 Reagents <br \/> A.2.1 Coulometric Karl Fischer reagent <br \/> A.2.2 Methanol (anhydrous) <br \/> A.2.3 Carrier gas <br \/> A.2.4 Water standard for Karl Fischer coulometric titration <br \/> A.3 Apparatus <br \/> A.3.1 Karl Fischer coulometric titration apparatus <br \/> A.3.2 Evaporator <br \/> A.3.3 Analytical balance <br \/> A.3.4 Sample container <br \/> A.3.5 Micro-syringe  <\/td>\n<\/tr>\n<tr>\n<td><b>17<b><\/td>\n<td>A.3.6 Dew-point hygrometer <br \/> A.4 Sampling  <br \/> A.5 Measurement steps <br \/> A.6 Test results <br \/> Figure A.1 \u2013 Sample container  <\/td>\n<\/tr>\n<tr>\n<td><b>18<b><\/td>\n<td>Table A.1 \u2013 Test data of water content in sample A  <\/td>\n<\/tr>\n<tr>\n<td><b>19<b><\/td>\n<td>Bibliography  <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"<p><b>Nanomanufacturing. Key control characteristics &#8211; Nano-enabled electrical energy storage. Determination of water content in electrode nanomaterials, Karl Fischer method<\/b><\/p>\n<table class=\"shortdes-table\" style=\"width: 100%\" border=\"0\" cellspacing=\"0\" cellpadding=\"0\">\n<tbody>\n<tr>\n<td>Published By<\/td>\n<td>Publication Date<\/td>\n<td>Number of Pages<\/td>\n<\/tr>\n<tr>\n<td><a href=\"https:\/\/pdfstandards.shop\/product-category\/publishers\/bsi\/\"><b>BSI<\/b><\/a><\/td>\n<td>2020<\/td>\n<td>20<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":302888,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[2641],"product_tag":[],"class_list":{"0":"post-302886","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-bsi","8":"first","9":"instock","10":"sold-individually","11":"shipping-taxable","12":"purchasable","13":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/302886","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/302888"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=302886"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=302886"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=302886"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}