{"id":302286,"date":"2024-10-19T20:39:01","date_gmt":"2024-10-19T20:39:01","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-iso-13547-22014\/"},"modified":"2024-10-25T18:09:41","modified_gmt":"2024-10-25T18:09:41","slug":"bs-iso-13547-22014","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-iso-13547-22014\/","title":{"rendered":"BS ISO 13547-2:2014"},"content":{"rendered":"

This International Standard specifies an acid digestion and inductively coupled plasma atomic emission spectrometric (ICP-AES) method for the determination of the mass fraction of arsenic in copper, lead, zinc, and nickel sulfide concentrates as follows:<\/p>\n

    \n
  1. \n

    for copper sulfide concentrates, the method is applicable to the determination of mass fractions of arsenic from 0,05 % to 2,0 %;<\/p>\n<\/li>\n

  2. \n

    for lead sulfide concentrates, the method is applicable to the determination of mass fractions of arsenic from 0,05 % to 1,0 %;<\/p>\n<\/li>\n

  3. \n

    for zinc sulfide concentrates, the method is applicable to the determination of mass fractions of arsenic from 0,05 % to 0,6 %;<\/p>\n<\/li>\n

  4. \n

    for nickel sulfide concentrates, the method is applicable to the determination of mass fraction of arsenic from 0,05 % to 1,0 %.<\/p>\n<\/li>\n<\/ol>\n

    PDF Catalog<\/h4>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
    PDF Pages<\/th>\nPDF Title<\/th>\n<\/tr>\n
    6<\/td>\nForeword <\/td>\n<\/tr>\n
    7<\/td>\nSection sec_1
    Section sec_2
    1\tScope
    2\tNormative references <\/td>\n<\/tr>\n
    8<\/td>\nSection sec_3
    Section sec_4
    Section sec_4.1
    Section sec_4.2
    Section sec_4.3
    Section sec_4.4
    Section sec_4.5
    Section sec_4.6
    Section sec_4.7
    Section sec_4.8
    Section sec_4.9
    Section sec_4.10
    Section sec_4.11
    Section sec_4.12
    Section sec_4.13
    Section sec_4.14
    Section sec_4.15
    Section sec_4.16
    3\tPrinciple
    4\tReagents <\/td>\n<\/tr>\n
    9<\/td>\nSection sec_4.17
    Section sec_4.18
    Section sec_4.19
    Section sec_4.20
    Section sec_4.21
    Section sec_4.22
    Section sec_4.23
    Section sec_4.24
    Section sec_4.25 <\/td>\n<\/tr>\n
    10<\/td>\nSection sec_4.26
    Section sec_5
    Section sec_5.1
    Section sec_5.2
    Section sec_5.3
    Section sec_5.4
    Section sec_5.5
    Section sec_6
    Section sec_6.1
    Section sec_6.2
    Section sec_6.3
    5\tApparatus
    6\tSampling and sample preparation
    6.1\tLaboratory sample
    6.2\tTest sample
    6.3\tTest portion <\/td>\n<\/tr>\n
    11<\/td>\nSection sec_7
    Section sec_7.1
    Section sec_7.2
    Section sec_7.3
    Section sec_7.4
    Section sec_7.5
    7\tProcedure
    7.1\tNumber of determinations
    7.2\tBlank test
    7.3\tDissolution of the test portion
    7.4\tRemoval of lead sulfate
    7.5\tDissolution of the insoluble residue <\/td>\n<\/tr>\n
    12<\/td>\nSection sec_7.6
    Section sec_7.7
    Table tab_1
    Section sec_7.8
    7.6\tPreparation of test solutions
    7.7\tPreparation of calibration solutions
    7.8\tPreparation of arsenic calibration curve <\/td>\n<\/tr>\n
    13<\/td>\nSection sec_7.9
    Section sec_8
    Section sec_9
    Section sec_9.1
    7.9\tDetermination of arsenic content in test solutions
    8\tExpression of results
    9\tPrecision
    9.1\tExpression of precision <\/td>\n<\/tr>\n
    14<\/td>\nSection sec_9.2
    Section sec_9.3
    9.2\tMethod for obtaining the final result
    9.3\tBetween-laboratories precision <\/td>\n<\/tr>\n
    15<\/td>\nSection sec_9.4
    Section sec_9.4.1
    9.4\tCheck of trueness <\/td>\n<\/tr>\n
    16<\/td>\nSection sec_9.4.2
    Section sec_9.4.2.1
    Section sec_9.4.2.2
    Section sec_9.4.2.3
    Section sec_10
    10\tTest report <\/td>\n<\/tr>\n
    17<\/td>\nAnnex sec_A
    Annex sec_A.1
    Annex sec_A.2
    Annex sec_A.3
    Annex sec_A.3.1
    Annex sec_A.4
    Annex sec_A.4.1
    Annex sec_A.4.2
    Annex sec_A.4.3
    Annex sec_A.5
    Annex sec_A.5.1
    Annex\u00a0A
    \n(normative)<\/p>\n

    Procedure for the preparation and determination of the mass of a pre-dried test portion <\/td>\n<\/tr>\n

    18<\/td>\nAnnex sec_A.5.2
    Annex sec_A.5.3
    Annex sec_A.6 <\/td>\n<\/tr>\n
    19<\/td>\nAnnex sec_B
    Figure fig_B.1
    Annex\u00a0B
    \n(normative)<\/p>\n

    Flowsheet of the procedure for the acceptance of analytical values for test samples <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"

    Copper, lead, zinc and nickel sulfide concentrates. Determination of arsenic – Acid digestion and inductively coupled plasma atomic emission spectrometric method<\/b><\/p>\n\n\n\n\n
    Published By<\/td>\nPublication Date<\/td>\nNumber of Pages<\/td>\n<\/tr>\n
    BSI<\/b><\/a><\/td>\n2014<\/td>\n22<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":302294,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[1053,2641],"product_tag":[],"class_list":{"0":"post-302286","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-73-060-99","7":"product_cat-bsi","9":"first","10":"instock","11":"sold-individually","12":"shipping-taxable","13":"purchasable","14":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/302286","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/302294"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=302286"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=302286"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=302286"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}