BS ISO 13322-1:2014
$167.15
Particle size analysis. Image analysis methods – Static image analysis methods
| Published By | Publication Date | Number of Pages |
| BSI | 2014 | 36 |
This part of ISO 13322 is applicable to the analysis of images for the purpose of determining particle size distributions where the velocity of the particles against the axis of the optical system of the imaging device is zero. The particles are appropriately dispersed and fixed in the object plane of the instrument. The field of view may sample the object plane dynamically either by moving the sample support or the camera provided this can be accomplished without any motion effects on the image. Captured images can be analysed subsequently.
This part of ISO 13322 concentrates upon the analysis of digital images created from either light or electron detection systems. It does not address the method of creating the image although the detection settings chosen together with its calibration are important to particle sizing accuracy. This part of ISO 13322 considers only image evaluation methods using complete pixel counts.
Both the type of distribution, (by number or by volume) together with the width of the particle size distribution has a very material influence upon the number of particles to be measured to secure the desired accuracy within the specified confidence limits. An example is shown in Annex A.
Automation of the analysis is possible in order to measure sufficient particle numbers for a required degree of precision.
This part of ISO 13322 does not address the sample preparation. However, the sub sampling, dispersion and presentation of particles to be measured are a vital part of the operational chain of actions necessary to ensure accuracy and precision of any final result.
NOTE Further details about sampling and sample preparation can be found in ISO 14887 and ISO 14488.
PDF Catalog
| PDF Pages | PDF Title |
|---|---|
| 6 | Foreword |
| 7 | Introduction |
| 9 | Section sec_1 Section sec_2 Section sec_3 Section sec_3.1 1 Scope 2 Normative references 3 Terms and definitions and list of symbols 3.1 Terms and definitions |
| 10 | Section sec_3.1.1 Section sec_3.1.2 Section sec_3.1.3 Section sec_3.1.4 Section sec_3.1.5 Section sec_3.1.6 Section sec_3.1.7 Section sec_3.1.8 Section sec_3.1.9 Section sec_3.1.10 Section sec_3.1.11 |
| 11 | Section sec_3.1.12 Section sec_3.1.13 Section sec_3.1.14 Table tab_a Figure fig_1 |
| 12 | Section sec_3.2 3.2 Symbols |
| 13 | Section sec_4 Section sec_4.1 Section sec_4.2 4 Preparation for image capture 4.1 Introduction 4.2 Procedures |
| 14 | Section sec_5 Section sec_5.1 Section sec_5.2 Section sec_5.3 Section sec_5.4 5 Sample preparation demands for method description 5.1 Sample splitting and reduction 5.2 Touching particles 5.3 Particle distribution 5.4 Number of particles to be counted |
| 15 | Section sec_5.5 Section sec_6 Section sec_6.1 Section sec_6.2 Section sec_6.2.1 5.5 Particle suspending fluid 6 Quality of captured images 6.1 General 6.2 Pixels per particle |
| 16 | Section sec_6.2.2 Section sec_7 Section sec_7.1 Section sec_7.2 7 Image analysis 7.1 General 7.2 Size classes and magnification |
| 17 | Section sec_8 Section sec_8.1 Section sec_8.2 8 Counting procedure 8.1 General 8.2 Particle image edges |
| 18 | Section sec_8.3 Section sec_8.3.1 Table tab_c Figure fig_2 Section sec_8.3.2 8.3 Particles cut by the edge of the measurement frame |
| 19 | Table tab_1 Section sec_8.3.3 Section sec_8.4 8.4 Touching particles |
| 20 | Section sec_8.5 Section sec_9 Section sec_10 Section sec_10.1 8.5 Measurements 9 Calculation of the particle size results 10 Calibration and traceability 10.1 General |
| 21 | Section sec_10.2 Section sec_10.2.1 Section sec_10.2.2 Section sec_10.2.3 10.2 Recommendations and requirements |
| 22 | Section sec_11 Section sec_11.1 Section sec_11.2 Section sec_11.3 11 Accuracy 11.1 General 11.2 Reference materials 11.3 Instrument preparation |
| 23 | Section sec_11.4 Section sec_11.5 Section sec_12 11.4 Qualification test 11.5 Qualification acceptance 12 Test report |
| 25 | Annex sec_A Annex sec_A.1 Annex sec_A.2 Annex sec_A.2.1 Table tab_A.1 Annex A (informative) Estimation of the number of particles to be counted for a given accuracy |
| 26 | Table tab_A.2 Annex sec_A.2.2 Annex sec_A.3 |
| 27 | Table tab_A.3 |
| 28 | Table tab_g Figure fig_A.1 |
| 29 | Table tab_h Figure fig_A.2 |
| 30 | Annex sec_B Annex sec_B.1 Annex sec_B.2 Annex sec_B.2.1 Annex sec_B.2.2 Annex B (informative) Common segmentation methods for particle edge detection |
| 31 | Annex sec_C Figure fig_C.1 Annex C (informative) Flow chart showing a typical image analysis method |
| 32 | Reference ref_1 Reference ref_2 Reference ref_3 Reference ref_4 Reference ref_5 Reference ref_6 Reference ref_7 Reference ref_8 Reference ref_9 Reference ref_10 Reference ref_11 Reference ref_12 Reference ref_13 Reference ref_14 Reference ref_15 Bibliography Bibliography |
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ISO 13322-1:2014
Particle size analysis — Image analysis methods — Part 1: Static image analysis methods Published…
