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BS EN 1302:1999:2002 Edition

$189.07

Chemicals used for treatment of water intended for human consumption. Aluminium-based coagulants. Analytical methods

Published By Publication Date Number of Pages
BSI 2002 46
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PDF Pages PDF Title
1 BRITISH STANDARD
2 National foreword
4 Foreword
Contents
5 1 Scope
2 Normative references
6 3 Preparation of the test sample
3.1 Definitions
3.1.1 laboratory sample
3.1.2 test sample
3.1.3 test portion
3.2 Procedure
4 Methods of analysis
Table 1 – Methods of analysis
7 Table 2 – Applicability methods of analysis
5 Expression of results
5.1 Aluminium content
5.2 Repeatability
8 Annex A (normative)
Reference methods of analysis
A.1 Determination of aluminium (EDTA complexometric method)
A.1.1 General
A.1.2 Principle
A.1.3 Reagents
9 A.1.4 Apparatus
A.1.5 Procedure
Table A.1
10 A.1.6 Expression of results
A.2 Determination of aluminium (CDTA complexometric method after separation of iron)
A.2.1 General
A.2.2 Principle
A.2.3 Reagents
11 A.2.4 Apparatus
A.2.5 Procedure
Table A2
12 A.2.6 Expression of results
13 A.3 Determination of iron (atomic absorption spectrometry)
A.3.1 General
A.3.2 Principle
A.3.3 Reagents
A.3.4 Apparatus
A.3.5 Procedure
14 Figure A.1 – Calculation of the iron concentration in the test solution
15 Figure A.2 – Calculation of the iron concentration in the blank solution
A.3.6 Expression of results
16 A.4 Determination of iron (total and Fe
A.4.1 General
A.4.2 Principle
A.4.3 Reagents
A.4.4 Apparatus
17 A.4.5 Procedure
A.4.6 Expression of results
18 A.5 Determination of sodium (atomic absorption spectrometry)
A.5.1 General
A.5.2 Principle
A.5.3 Reagents
A.5.4 Apparatus
19 A.5.5 Procedure
20 Figure A.3 – Calculation of the sodium concentration in the blank solution
21 A.5.6 Expression of results
A.6 Determination of calcium (atomic absorption spectrometry)
A.6.1 General
A.6.2 Principle
A.6.3 Reagents
A.6.4 Apparatus
22 A.6.5 Procedure
23 Figure A.5 Calculation of the calcium concentration in the blank solution
24 A.6.6 Expression of results
A.7 Determination of chloride (potentiometric method)
A.7.1 General
A.7.2 Principle
A.7.3 Reagents
A.7.4 Apparatus
A.7.5 Procedure
25 Table A.3 – Dilutions and aliquot portion
A.7.6 Expression of results
A.8 Determination of sulfate (gravimetric method)
A.8.1 General
A.8.2 Principle
26 A.8.3 Reagents
A.8.4 Apparatus
A.8.5 Procedure
Table A.4 – Aliquot portion
27 A.8.6 Expression of results
A.9 Determination of silicate (reduced molybdosilicate spectrometric method)
A.9.1 General
A.9.2 Principle
A.9.3 Reagents
A.9.4 Apparatus
A.9.5 Procedure
28 Table A.5 – Dilutions and aliquot portion
A.9.6 Expression of results
A.10 Determination of free acidity (titrimetric method)
A.10.1 General
A.10.2 Principle
29 A.10.3 Reagents
A.10.4 Apparatus
A.10.5 Procedure
Table A.6 – Aliquot portion
30 A.10.6 Expression of results
31 A.11 Determination of basicity (titrimetric oxalate method)
A.11.1 General
A.11.2 Principle
A.11.3 Reagents
A.11.4 Apparatus
A.11.5 Procedure
Table A.7 – Aliquot portion for basicity, titrimetric oxalate method
32 A.11.6 Expression of results
33 A.12 Determination of basicity (titrimetric potassium fluoride method)
A.12.1 General
A.12.2 Principle
A.12.3 Reagents
A.12.4 Apparatus
A.12.5 Procedure
34 Table A.8 – Aliquot portion
A.12.6 Expression of results
35 A.13 Determination of insoluble matter (gravimetric method)
A.13.1 General
A.13.2 Principle
A.13.3 Reagents
A.13.4 Apparatus
A.13.5 Procedure
36 A.13.6 Expression of results
A.14 Determination of cadmium (Cd), chromium (Cr), nickel (Ni) and lead (Pb) [inductively coupled plas…
A.14.1 General
A.14.2 Principle
A.14.3 Reagents
A.14.4 Apparatus
37 A.14.5 Procedure
38 Figure A.7 – Calculation of the metal concentration in the test solution
Figure A.8 – Calculation of the metal concentration in the blank solution
39 A.15 Determination of arsenic (As), selenium (Se) and antimony (Sb) by ICP-OES (hydride�technique)
A.15.1 General
A.15.2 Principle
A.15.3 Reagents
40 A.15.4 Apparatus
A.15.5 Procedure
41 A.16 Determination of mercury (cold vapour atomic absorption spectrometry)
A.16.1 General
A.16.2 Principle
A.16.3 Reagents
42 A.16.4 Apparatus
A.16.5 Procedure
A.16.6 Expression of results
43 Annex B (informative)
Routine methods
B.1 General
B.2 Methods for metals other than aluminium
B.3 Evaluation of relative basicity (calculation method)
B.3.1 General
B.3.2 Principle
B.3.3 Procedure
44 B.3.4 Expression of results
B.3.5 Calculated relative basicity
45 Annex C (informative)
Bibliography
BS EN 1302:1999
$189.07