{"id":315517,"date":"2024-10-19T21:44:55","date_gmt":"2024-10-19T21:44:55","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-en-15199-42015\/"},"modified":"2024-10-25T19:53:22","modified_gmt":"2024-10-25T19:53:22","slug":"bs-en-15199-42015","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-en-15199-42015\/","title":{"rendered":"BS EN 15199-4:2015"},"content":{"rendered":"

This European Standard describes a method for the determination of the boiling range distribution of petroleum products by capillary gas chromatography using flame ionization detection. This European Standard is applicable to stabilized crude oils and for the boiling range distribution and the recovery up to and including n-nonane. A stabilized crude oil is defined as having a Reid Vapour Pressure equivalent to or less than 82,7 kPa as determined by IP 481 [3]<\/span>.<\/p>\n

\n
\n NOTE\n <\/div>\n

For the purposes of this European Standard, the terms  \u201c<\/i>% (m\/m)\u201d<\/i> and  \u201c<\/i>% (V\/V)\u201d<\/i> are used to represent respectively the mass fraction, \u03c9<\/i>, and the volume fraction, \u03c6<\/i>.<\/p>\n<\/div>\n

\n
\n WARNING\n <\/div>\n

The use of this European Standard can involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to take appropriate measures to ensure safety and health of personnel prior to application of the standard, and fulfil statutory and regulatory requirements for this purpose.<\/b><\/p>\n<\/div>\n

PDF Catalog<\/h4>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
PDF Pages<\/th>\nPDF Title<\/th>\n<\/tr>\n
5<\/td>\nEuropean foreword <\/td>\n<\/tr>\n
6<\/td>\n1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents and materials <\/td>\n<\/tr>\n
7<\/td>\n6 Apparatus
6.1 Analytical balance
6.2 Gas chromatograph
6.3 Detector
6.4 Pre-column configurations
6.4.1 Heated valve switching box (see Figure B.1) <\/td>\n<\/tr>\n
8<\/td>\n6.4.2 Injection port (see Figure B.2 and B.3)
Table 1 \u2014Typical chromatographic conditions
6.5 Analytical column
6.5.1 General <\/td>\n<\/tr>\n
9<\/td>\n6.5.2 Resolution
Figure 1 \u2014Determination of resolution
6.6 Skewness <\/td>\n<\/tr>\n
10<\/td>\nFigure 2 \u2014Calculation of peak skewness
6.7 Data collection
7 Sampling and sample handling
8 Calculation of response factors <\/td>\n<\/tr>\n
11<\/td>\nTable 2 \u2014 Calculated response factors for hydrocarbons
9 Procedure
9.1 Sample preparation
9.2 Determination of backflush time
9.2.1 Initial work
9.2.2 Analytical column
9.2.3 Accelerated analytical column <\/td>\n<\/tr>\n
12<\/td>\nFigure 3 \u2014 Example chromatogram showing elution for determining backflush time
9.3 Sample analysis
9.3.1 Initial work
9.3.2 Calculation of individual components results <\/td>\n<\/tr>\n
13<\/td>\n9.3.3 Boiling point distribution of fraction up to and including nonane
10 Reporting
11 Precision
11.1 General
11.2 Repeatability, r
11.3 Reproducibility, R <\/td>\n<\/tr>\n
14<\/td>\n12 Test report <\/td>\n<\/tr>\n
15<\/td>\nAnnex A (informative) Analysis assistance
Table A.1 \u2014 Example report of an analysis <\/td>\n<\/tr>\n
20<\/td>\nFigure A.1 \u2014 Example chromatograms belonging to report data of Table A.1 <\/td>\n<\/tr>\n
21<\/td>\nAnnex B (informative) Apparatus configuration
Figure B.1 \u2014 Typical configuration using a heated valve switching box <\/td>\n<\/tr>\n
22<\/td>\nFigure B.2 \u2014 Typical configuration with direct connection to the capillary column
Figure B.3 \u2014 Typical configuration with a connection via a splitter to the capillary column <\/td>\n<\/tr>\n
23<\/td>\nBibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"

Petroleum products. Determination of boiling range distribution by gas chromatography method – Light fractions of crude oil<\/b><\/p>\n\n\n\n\n
Published By<\/td>\nPublication Date<\/td>\nNumber of Pages<\/td>\n<\/tr>\n
BSI<\/b><\/a><\/td>\n2015<\/td>\n26<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":315524,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[2641],"product_tag":[],"class_list":{"0":"post-315517","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-bsi","8":"first","9":"instock","10":"sold-individually","11":"shipping-taxable","12":"purchasable","13":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/315517","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/315524"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=315517"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=315517"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=315517"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}