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BS EN IEC 60754-3:2019

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Test on gases evolved during combustion of materials from cables – Measurement of low level of halogen content by ion chromatography

Published By Publication Date Number of Pages
BSI 2019 28
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This part of IEC 60754 specifies the apparatus and procedure for the measurement of the amount of halogens evolved during the combustion of materials taken from electric or optical fibre cable constructions.

The method specified in this document is intended for the measurement of the content of chlorine (Cl), bromine (Br), fluorine (F) and iodine (I), by using the analytical technique of ion chromatography for analysing an aqueous solution resulting from the gases evolved during the combustion.

The heating (combustion) procedure in this part of IEC 60754 is the same as in IEC 60754-2.

The method is intended for materials with an individual halogen content not exceeding 10 mg/g.

The method specified in this document is intended for the testing of individual components used in a cable construction. The use of this method will enable the verification of requirements which are stated in the appropriate cable specification for individual components of a cable construction.

NOTE 1 The relevant cable standard indicates which components of the cable are tested.

NOTE 2 This test method is sometimes used to test materials to be used in cable manufacture.

For reasons of precision, this method is not recommended for detecting values of halogens less than 0,1 mg/g of the sample taken.

PDF Catalog

PDF Pages PDF Title
2 undefined
7 English
CONTENTS
9 FOREWORD
11 INTRODUCTION
12 1 Scope
2 Normative references
3 Terms and definitions
13 4 Test method principle
5 Test apparatus
5.1 General
5.2 Tube furnace
14 5.3 Quartz glass tube
5.4 Combustion boat
5.5 Bubbling devices for gases
15 5.6 Air supply system
5.7 Analytical balance
5.8 Laboratory glassware
16 5.9 Ion chromatographic system
6 Test specimen
6.1 General
6.2 Conditioning of specimen
6.3 Mass of specimen
7 Test procedure
7.1 General
17 7.2 Blank test
7.3 Test apparatus and arrangement
7.4 Heating procedure
7.5 Washing procedure
7.6 Measurement of the halogens
18 8 Evaluation of the test results
9 Performance requirement
10 Test report
19 Figures
Figure 1 – Device for inserting combustion boat and test specimen
20 Figure 2 – Example of a gas washing bottle
21 Figure 3 – Test apparatus: method 1 – Use of synthetic or compressed air from a bottle
22 Figure 4 – Test apparatus: method 2 – Use of laboratory compressed air supply
23 Figure 5 – Test apparatus: method 3 – Use of ambient air sucked by means of a suction pump
24 Figure 6 – Example of ion chromatographic system
25 Annex A (informative)Recommended use and performance requirements
A.1 Recommended use
A.1.1 General
26 A.1.2 Recommended use of IEC 60754-1, IEC 60754-2 and IEC 60754-3
A.2 Recommended performance requirements to assess materials described as “halogen free”
Table A.1 – Scope and recommended use of IEC 60754-1,IEC 60754-2 and IEC 60754-3
Table A.2 – Recommended performance requirements to assess materialsdescribed as “halogen free”
27 Bibliography
BS EN IEC 60754-3:2019
$142.49